High Temperature X‐Ray Diffraction Techniques for Active Metals

High-temperature spreading kinetics of metals

A High-temperature Powder Diffraction Furnace

A new high-temperature XRD instrument, utilizing multilayer optics and a custom furnace, has been developed to maximize sensitivity and minimize problems associated with sample displacement. This paper will describe the technical specifications of the new instrument, and will present temperature calibration with standard reference materials and measurement of phase evolution in an industrial gl...

Precious Metals in High Temperature Geothermal Systems

High temperature geothermal systems are the modern analogue of epithermal precious metal ore deposits. In these systems, gold and silver are transported primarily as bisulfide complexes, with the precious metals being deposited in response to boiling and mixing of the deep geothermal fluid. In order for the geothermal system to produce an economic precious metal deposit within the typical lifet...

High temperature X-ray diffraction apparatus.

High Pressure-High Temperature, X-Ray Diffraction Apparatus

A tetrahedral-anvil press has been developed that permits x-ray diffraction powder measurements at pressures to 75 kb and temperatures to 1000°C. A counting technique, rather than photographic film, is used for x-ray detection. Sample tetrahedra of compressed LiH, boron, and boron-filled plastic are used in place of the pyrophyllite customarily used for this purpose. Two possible entrance pupil...